ISO 13162:2021 水质 碳14 使用液体闪烁计数的试验方法

标准编号:ISO 13162:2021

中文名称:水质 碳14 使用液体闪烁计数的试验方法

英文名称:Water quality — Carbon 14 — Test method using liquid scintillation counting

发布日期:2021-06

标准范围

本文件规定了一种通过液体闪烁计数(LSC)直接在测试样品上或在化学分离后测量所有类型水样中14C活度浓度的方法。该方法适用于供应/饮用水、雨水、地表水和地下水、海水以及冷却水、工业用水、生活和工业废水的测试样品。检测限取决于样品体积、使用的仪器、样品计数时间、背景计数率、检测效率和化学回收率。本文所述的方法,采用目前可用的液体闪烁计数器和合适的技术条件,检出限低至1?Bq?l?1,低于WHO饮用水安全饮用标准(100?Bq·l-1).14C活度浓度可高达106?Bq?l-1,无任何样品稀释。用户有责任确保本测试方法对所测试水样的有效性。

This document specifies a method for the measurement of 14C activity concentration in all types of water samples by liquid scintillation counting (LSC) either directly on the test sample or following a chemical separation.

The method is applicable to test samples of supply/drinking water, rainwater, surface and ground water, marine water, as well as cooling water, industrial water, domestic, and industrial wastewater.

The detection limit depends on the sample volume, the instrument used, the sample counting time, the background count rate, the detection efficiency and the chemical recovery. The method described in this document, using currently available liquid scintillation counters and suitable technical conditions, has a detection limit as low as 1 Bq?l?1, which is lower than the WHO criteria for safe consumption of drinking water (100 Bq·l-1). 14C activity concentrations can be measured up to 106 Bq?l-1 without any sample dilution.

It is the user’s responsibility to ensure the validity of this test method for the water samples tested.

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